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Simultaneous ICP-OES

Simultaneous ICP-OES

Simultaneous ICP-OES 3000 Application fields Silicon Industrial: magnetic materials Metallurgical: analyze As, Bi, Pb, Sb, Sn and other impurity elements,which effect greatly the metallic materials quality Water analysis: analyze 8 heavy metal elements Geological, minera: analyze Ca, Mg, Na, Fe,...

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Product Details

Simultaneous  ICP-OES 3000
Application fields
Silicon Industrial: magnetic materials
Metallurgical: analyze As, Bi, Pb, Sb, Sn and other impurity elements,which effect greatly the metallic materials quality
Water analysis: analyze 8 heavy metal elements
Geological, minera: analyze Ca, Mg, Na, Fe, Cu, Mn, Zn, Co, Ni, Au, Ag and other elements in the rock samples
Petrochemical and Industrial: Analyze over 30 elements in crude oil, mainly Fe, Na, Mg, Ni, V, Ca, Pb, Mo, Mn, Cr, Co, Ba, As, etc.
Pharmaceutical, health, agricultural and environmental and Food safety

ICP-3000 Simultaneous ICP-OES spectrometer is a powerful performance, simultaneous full-spectrum direct-reading spectrometer developed by Skyray Instrument, which is used for trace elemental analysis in diverse samples (soluble in hydrochloric acid, nitric acid, hydrofluoric acid,etc). The instrument offers capabilities with automatization, stability, reliability and ease of use.

Technical parameters
RF Generator Technical Specifications
Input Power:AC 220V, 20A
Output power:700~1600W 
Working Frequency:27.12MHz 
Frequency stability:<0.05% 
Output power stability:<0.1% 
Match method:auto-matching
Electromagnetic leakage radiation intensity:electric field intensity E <0.5V / m at 30cm away from the chamber
Introduction sample system technical specifications
Output coil:Inner-diameter 25mm, 3 turns 
Quartz tri-concentric torch: Outer-diameter 20mm. Various center channel size models optional
High-efficient nebulizer: Concentric nebulizer outer-diameter 6mm. Vvarious models ( high-salt, anti-HF, etc.)optional
Scott spray chamber, the cyclonic spray chamber with outer diameter 57.2mm optional 
Peristaltic pump:12-roller, 4-channel, the rotation speed can be adjusted according to the demanded flow 
Argon flow meter/carrier gas pressure gauge specifications:Plasma gas flow meter (100-1000)L/h (1.6-16L/min), Auxiliary gas flow meter(6-60)L/h (0.1-1L/min), Carrier gas flow meter(6-60)L/h (0.1-1L/min), Carrier gas regulator valve (0.2MPa), Cooling water: Water temp. 20-25ºC Flow> 5L/min Pressure> 0.1MPa

Simultaneous ICP-OES spectrometer specifications
Ruled echelle grating:52.67 lp/mm, 64°blaze angle, the substrate is made of the Zerodur? produced by German SCHOTT, features near-zero thermal expansion coefficient ,enabling outstanding performance
Prism:Ultra-pure Corning UV fused silica, transmittance 99.6% at 170nm.
Wavelength range:175nm~900nm for standard, extended to 165nm-900nm by choosing DUV optical components
Effective Focal length:430mm
Numerical aperture:F/8, ultra-high flux ensures the instrument detection limit and sensitivity
Stray light:Equivalent background concentration of 10000ppmCa solution <2ppm at As189.042nm
Optical chamber:Precisely thermostat, 35±0.1ºC Distributed N2 purge: normal purge 2L/min, fast purge 4L/min

Detection device Technical Specifications
Detector Type:Charge injection detector (CID) 
Pixel Size:27 x 27 μm,Random Access Integration (RAI)
Read mode:Full frame readout (FF), Random Access Integration (RAI) with non-destructive read (NDRO) 
Linear dynamic range:108
Wavelength response range:165nm-1000nm
Electronic shutter:Set the integration time of each line; specify the individual line to read out(read time <2ms)
Quantum efficiency:No coating, up to 35% within 200nm UV region
Detector cooling:High efficiency triple stage thermoelectric cooling device maintains the detector at a constant - 45 ºC

Simultaneous ICP-OES Specifications
View mode:Radial view
Liquid content:0.01ppm- several thousands ppm
Solid content:0.001%-70%
Repeatability:(short-term stability) relative standard deviation RSD <0.5%
Stability:Relative standard deviation RSD <1% within 2 Hours
Analysis speed:Single line CID readout time is 2ms, analysis for all elements can be achieved within one minute
Detection limit (μg/L):1ppb-10ppb for most elements
Instrument size:Desktop1300mm*840mm*740mm

Simultaneous ICP-OES Advantages
Full automation design
The instrument is thoroughly computer-controlled except the power switch, which is reliable, safe and convenient.
Peristaltic pump
A high precision 12 roller, 4 channel peristaltic pump, with speed adjustable according to the demanding, provides smooth, stable sample introduction and drain, to ensure the introduction rate consistent with the drain rate, which is adjusted as per required to stabilize the introduction system.
Auto-control of gas flow
In the sample introduction system, the carrier gas, plasma gas, auxiliary gas are controlled through the advanced mass flow controller (MFC), features continuously adjustable and stable, etc., which ensures the stability of the introduction system and the foundation for the stable light source.
Precise wavelength positioning
Intelligent, precise automatic wavelength calibration algorithm, achieves the measurement without additional peaks calibration, to ensure an accurate measurement whilst saving solution and measurement time.
Fast, accurate auto-matching
The load terminals employs the full-automatic matching technology developed by Jiangsu Skyray Instrument Co.,Ltd., features fast matching, high precision, etc., which could achieve maximum output power, enhance power efficiency, ensure the stability of the instrument whilst facilitating ignition.
Ultra-fast analysis speed
The analyst can set any suitable integration time for all the analytical lines in one exposure to achieve optimal measurement, or acquire the intensity integral value in the end of the exposure to enable the analysis faster, or specify any one or several specific line(s)to read-out(the readout time<2ms).
Powerful software analysis function 
Software is easy to operate and intuitive, it offers the capability with qualitative, semi-quantitative and quantitative analysis, instrument diagnostics, intelligent optimization, flexible full-spectrum research function, strong offline reprocessing, scientifically intelligence background correction and interference cancellation algorithm, which enable the analysis more professional and accurate.
Advanced sample introduction system
The sample introduction system is efficient and stable, equipped with various nebulizers and spray chambers, it can also be equipped with high solids nebulizer, hydrogen fluoride-resistant nebulizer, per required. Besides, the autosampler developed by Skyray facilitates the operation, and further improves the analysis efficiency.
Stable, advanced solid-state RF power
The instrument employs the solid-state RF power developed by Jiangsu Skyray Instrument Co., Ltd., which is compact and delivers reliable performance with the power stability and safety, to further improve the instruments stability and security.
Superb optical system
Adopting the echelle-prism cross-dispersion type polychromator, elegant optical optimization design maximizes the flux whilst enabling the excellent spectral resolution. No movable optical components achieves unparalleled long-term stability; Ultra-low stray light design with the unique optical design greatly reduces the background interference and further improves the detection limit. A highly efficient N2 distributed purge system for the optical tank combined with the high-quality optics ensures deep UV analysis, especially P, S, As, etc..
Excellent performance detector
Employing the CID detector, which is advanced, mature and stable, largest-size active area, megapixel. Full-frame Imaging ability to capture the entire ICP-OES spectrum (165-900 nm) permits quantitative analysis. Non-destructive readout improves the signal-to-noise ratio of weak analyte lines and ensures the precision of results, whist enabling data acquirement and analysis faster than CCD. Excellent linear dynamic range and inherent anti-blooming capability allow the measurement of weak analyte emission signals adjacent to intense emission signals, whilst providing flexibility to choose the ideal wavelength for a method (alternative secondary and tertiary lines to overcome interferences).

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